TTST OF CONTENT

SECTION I : ADMINISTRATTVEPART

Sample collection control form (995474)

Docurnentation^ofShipping {E-AR-02)

Documentation ofjeceipt of intact sample

Mails from : US'ADAAJCI/LNDD/CPLD/Dr. De Boer

Staff involved in the B analysis

Acknowlegment of receipt of A sample documentation package

Opening form of sanq)le B

Internal chain of custudy of A and B samples and aliquots

SECTION 2 : TECHNICAL FART

' C/ A L'ORIGINAL

pages 1-31

Pages 1 and 2
Page 3
Page 4
Pages 5 to 22
Page 23
Page 24

Pages 25 and 26
Pages 27 to 3!

pages 32 -134

2 1 Analysis for confirmation of T/E ratio

List of confirmation analyses, method and preparative form, descnption of analysis

Analysis program
Calibration curves

- Negative aliquot

- Sample B 995474 aliquots {N-3 with hydrolysis; N=l without hydrolysis)

- Positive aliquots
Result form

Data on instniment performances

Page 32 to 43
Page 44

Pages 45 and 46
Pages 47 and 48
Pages 49 to 56
Pages 57 to 59
Page 60
Pages 61 to 64

I ;

^j

2.2, Confirmation analysis hy GC/C/IRMS

List of confimiation analyses, method and preparative fom

2.2.1. GC/MS analysis

Description of GC/MS analysis

Analysis program

GC/MS analysis data: Negative aliquot and Sample B995474 for each fraction

Result form

Data on instrument performances

Pages 65 to 73

Pages 74 to 78
Page 79
Pages 80 to 93
Pages 94 to 96

Pages 97 to 99

Pages 100 to 101

2.2.2, Isotopic ratio analysis

Descnption of GC/C/IRMS analysis , ,^^, ,-,■,

Isotopic mtio analysis data: Negative aliquot and Sample B995474 for each fraction Pages 02 to 21

n f. ^ Pages 122 to 123

Result form "

Data on instrument performances ^^8^^ '■^^ ^^ '-*^

SECTION 3 : Certiricate of analysis n°28541

pages 135-136

ANNEXES

Comments from Dr Douwe de Boer
List of the requests from Dr. Douwe de Boer

pages 137-139

Pages 137 to 138
Page 139

USADA 0225