Quantification du rapport T/E

Calibration Last Updated: Mon Jul 24 12:54:54 2006

Reference Window: 2.00 Minutes
Non-Reference Window: 1.00 Minutes
Correlation Window: 0.10 minutes
Default Multiplier: 1.00
Default Sample Concentration: 0.0

Compound Information

1) Methyltestosterone (ISTD TR)

Ret. Time 20.92 min. , Extract & Integrate from 20.42 to 21.42 min.

Signal Rel Resp. Pet. Unc. (rel) Integration
Tgt 301.30 man27.e

Lvl ID Cone (ng/mL) Response

1 100.000 4680010

2 100.000 4212735

3 100.000 5428625

Qualifier Peak Analysis ON ISTD cone: 100.000 ng/mL
Curve Fit : Linear

2) Epitestosterone ( )

Ret. Time 18.51 min., Extract & Integrate from 18.01 to 19.01 min.

Signal Rel Resp. Pet. Unc. (rel) Integration
Tgt 432.40 man27.e

Lvl ID Cone (ng/mL) Response

1 5.000 181309

2 30.000 1100720

3 60.000 3350917

Qualifier Peak Analysis ON

Curve Fit: Linear, forced through origin

3) testosterone I )

Ret. Time' 19.31 min., Extract & Integrate from 18.81 to 19.81 min.

Signal Rel Resp. Pet. Unc. (rel) Integration
Tgt 432.40 man27.e

Lvl ID Cone (ng/mL) Response

1 30.000 1359912

2 180.000 7964015

3 360.000 21495301

Qualifier Peak Analysis ON

Method: MAN27.M Mon Jul 24 12:55:02 2006 Page:2

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