Quantification T/E (3 points) Calibration Last Updated: Mon Jul 24 17:15:46 2006 Reference Window: 2.00 Minutes Non-Reference Window: 1.00 Minutes Correlation Window: 0.10 minutes Default Multiplier: 1.00 Default Sample Concentration: 0.00 Compound Information 1) 17methyltestosterone (ISTD TR) Ret. Time 20.94 min. , Extract & Integrate from 20.44 to 21.44 min. Signal Rel Resp. Pet. Unc . (rel) Integration Tgt 301.30 man27.e Lvl ID Cone (ng/ml) Response 1 100.000 5915926 2 100.000 4981326 3 100.000 5130998 Qualifier Peak Analysis ON ISTD cone : 100.000 ng/ml Curve Fit : Linear 2) epitestosterone ( ) Ret. Time 18.52 min., Extract & Integrate from 18.02 to 19.02 min. Signal Rel Resp. Pet. Unc. (rel) Integration Tgt 432.40 man27.e Lvl ID Cone (ng/ml) Response 1 5.000 234336 2 30.000 1211449'. 3 60.000 2929592- Qualifier Peak Analysis ON Curve Fit: Linear, forced through origin 3) testosterone ( ) Ret. Time 19.32 min., Extract & Integrate from 18.82 to 19.82 min. Signal Rel Resp. Pet. Unc. (rel) Integration Tgt 432.40 man27.e Lvl ID Cone (ng/ml) Response 1 30.000 1557516 ' 2 180.000 7052377- 3 360.000 17023691- Qualifier Peak Analysis ON Method: MAN27.M Mon Jul 24 17:15:54 2006 Paqe:2 USADA 0086