^'1

Fri Jul 21 10:50:37 2006
C : \MSDCHEM\ l\5973N\atune . u
Mass 69.10 r Mass
Ab 402237 Ab
Pw50 O.Gl PwSO

I

5973N Autotune

Instrument; GC MSD

219.00

353944

0.60

Mass 502.10
Ab 70474
PwSO 0.59

'•A.

Ion Pol

Emission

EIEnrgy

Filament

Repeller
lonFcus
EntLens
EntOffs

PFTBA

POS MassGain -les
MassOffs -11
34 . G AmuGain
69.9 AmuOffs
2 Wid219
DC Pol
34.81
90.2 HEDEnab
9.5 EMVolts
18.32

Samples 8

OPEN Averages 3

Stepsize o.io

1830

135

-0.038

POS

ON

171B

Zones :
MS Source
MS Quad

230 Foreline
150

66

71

216

221

500

505

Scan: 10.00 - 700.00 Samples: B Thresh: 100 Step: 0.10

137 peaks Base: 69.00 Abundance: 387776

100

80 -

60

40

20

.^J...

.■ I ,■> ' >

100

200

300

400

500

600

Mass Abund Rel Abund Iso Mass Iso Abund Iso Ratio

69.00 387776 100.00 70.00 4355 1 12

219.00 341120 87.97 220.00 14592 4.26

502.00 67320 L7.36 503.00 6523 9.69

Air/Bater "uneck: H20-0.&S%/ N2-J .61* 02-1. 00* — C02-Q.i6% M2/HS6~3eO.S 7 t
Column Flow; Front: 1.324 Back: ml/min. Interface Temp: 300

Ramp Criteria:

Ion Focus Maximum
Repeller Maximum

90 volts using ion 502;
35 volts using ion 219;

EM Gain 80957
MassGain Values ©Samples: -18703 -17902 -17181 -157®0 -113@PS

72

TARGET MASS: 50 69 131 219

Amu Offset: 135.0 135.0 135.0 135.0
Entrance Lens Offset: IB. 3 18.3 18.3 18.3

414

135.0
18.3

502

135.0
18.3

800

135.0
18.3

USADA 0065

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