C:\MSD18\JUILLET06\2107\21rclO3.D\da File: Operator: Date Acquired: 21 Jul 06 12:59 pm Instrument; GC MSD Method File: MAN06B_B.M Sample Name: 2107 rcl 028 2007 HI ' Misc Info: Vial Number : i ^r^M , .,,>., ^"^ Pregnanediol llKetoetiocholanolone -bundancelon 434.40 (434.10 Abundancelon _432_.40 (432.10 Abundanceion 117.10 (116.80 Abundancelon 343.30 (343.00 )4.j|l24 3000' 20001 1000 '14.217 I i 10000 5000 13*52 W ..„ Trme-> 14.00 60000 60000 40000 20000 17i96 I 14.86 Time-> 13.40 / A , , 8000 i 6000 4000 2000 'T 14.10 Time"> 17.00 17.B6 Time~> 14.00 14.86 3b Androstandione 4 Androstenedione Inhib derivation 3a-5 Cyclo ^bundancelon 432.40 (432.10 Abundancelon 430,40 (430,10 Abundancelon 361,30 (361.00 Abundancejon432,40(432,10 1000 500 100 50 .'ime-> 10.30 11,60 Time-> 14.00 300 200 TOO r^ it^NfM 40 20 15,30 Time-> 5,50 6.00 Tf[ne-> 9,00 Page 2/16 USADA 0062 <=;:i