C:\MS D1 BUUlLLETaE\2107\21rcl03.D 5ata File Path C:\MSDiBUUiLLET06\2ion Data File Name 21rcl03.D Operator Acq. Method File MAN06B_B.M Sample Name 2107 rcl 028 2007 HI Misc Info Vial Number 1 Instrument Name GC MSD Calibration Title Calibration des steroides endogenes Last Calibration Update Fri Jui 21 13;26:58 2006 FictiJer recal utilise 21rcl03.D # Peak Type Ret Time Signal Name 1) •ISTD 16.99 301.3 Methyltestosterone 2) 12.21 438.4 Andro -D4 glue 3) 4,08 372.3 Salbutamol -03 4) 12.22 434.4 Androsterone 5) 12.47 434.4 Etiocholanolone 6) 12.61 241.2 5a3a diol 7) 12.77 241.2 5b38 dioi 8) 17.60 117.1 Pregnanediol 9) 0.00 434.4 DHT 10) 13.65 432.4 DHEA 11) 14.22 432.4 Epilestosterone 12) 15.10 432.4 Testosterone 13) 17.36 371.3 THC-M 14) 4.10 369.3 Salbutamol 15) 15.83 522.5 11 bOH Etiocholanolone 16) 21.29 548.5 THS 17) 22.04 636.6 THF 18) 22.80 632.6 Cortisol 19) 14.57 343.3 1 1 Keloetiocholanonlone 20) 0.00 432.4 3a-5C Date:.^41.U&,. Operateur ; ...23::.. CM Resultats : Hcn Ndgatif A verifier [] Remarques : Target Response Amount 1,587,292 200 62,992 125 472,321 100 9,682,254 2000 9,908,352 2000 268,022 100 257,498 100 4,046,186 400 457,571 100 446.439 40 498,991 40 49,013 15 443.177 94 923,980 200 585,640 50 16,444,095 1500 473.452 50 369.571 100 Units ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml ng/ml Ad4glu/Si'100 T/ET Testosterone Epitestosterona Androsterone Etiocholanolone DHEA DHT Andro / Etio 5a3a / 5b3a diol [Surface] THC -M Salb/Salb 03 ' 100 Cortisol / THS THF / THS 11 bOH etio /THS THF Sr/3a5c 4.0 1.1 [concentration] 1.0 1.0 94 #DIV/0! 40.0 40.0 2,000 2,000 100 15.0 93.9 1.0 30.0 4.0 1500 Valeurs conventionnelles de relet Rapport Concentration Concentration Concentration Rapport Rapport Concentration Concentration <19.1 >4 >200 >200 Concentration > 10000 Concentration > 10000 Concentration >200 Pour info (R&D) >20 >3 >2 >15 >75 USADA 0060 5!