C:\US D1 StJuilletaSV2107\21 hDS.D Data File Path C:\MSDlB\jullletO6\2107\ Data File Name 21h08.D Operator m37p35 Acq. Method File MAN06B_B.M Sample Name 178/07 995474 H Misc Info Viai Number 11 Instrument Name GC MSD Calibration Title Calibration des stiroides endogfines Last Calibration Update Fri Jul 21 13:26:58 2006 Fichier recal utilise 21rcl03.D Date:..22.t(Xtr. Op6rateur : C[ ] R6sultats : Renjauiiies :i J_nh\.bv.; r^: HC[] N^gatif A verifier T :i.C\e.. [] # 1) 2) 3) 4) 5) 6) 7} 8} 9) 10) 11) 12) 13) 14) 15) 16) 17) 18) 19) 20) Peak Type Ret Time Signal Name Target Response Amount Units •ISTD 17.09 301.3 Mettiyltestosterone 1,209.250 200 ng/ml 12.27 438.4 Andro -D4 glue 62,604 163 ng/ml 4.22 372.3 Saibutamol -D3 814,633 226 ng/ml 12,30 434.4 Androsterone 846,467 230 ng/ml 12.52 434.4 Etiocholanolone 813,037 215 ng/ml 12.70 241.2 5a3a diol 197,002 96 ng/ml 12.88 241.2 5b3a diol 439,619 224 ng/ml 17.85 117.1 Pregnanediol 10,142,344 1316 ng/ml 0.00 434.4 DHT ng/ml 0.00 432.4 DHEA ng/ml 14.30 432.4 Epitestosterone 116,467 14 ng/ml 15.20 432.4 Testosterone 575,745 61 ng/ml 0.00 371.3 THC-M ng/ml 0.00 369.3 Saibutamol -45 ng/ml 0.00 522.5 1 1 bOH Etiocholanolone ng/ml 0.00 548.5 THS ng/ml 0.00 636.6 THF ng/ml 0.00 632.6 Cortisol ng/ml 14.68 343.3 1 1 Keloetiocholanonlone 183,640 65 ng/ml 10.25 432.4 3a-5C 23,035 ng/ml [Surface] [concentration] Valeurs conventlonnelles de relet Ad4a)u/SI*100 5.2 <19.1 T/ET Testosterone Epitestosterone 4.9 60.6 13,7 Rapport > 4 Concentration > 200 Concentration >200 Androsterone Etiocholanolone DHEA 230 215 Concentration > 10000 Concentration > 10000 Concentration > 200 DHT Andro / Etlo 5a3a / 5b3a diol 1.0 0.4 Concentration > 20 Rapport > 3 Rapport > 2 THC -M Salb/SalbD3M00 0.0 ■45.0 Concentration >15 Concentration > 75 Cortisol /THS THF/THS 11 bOHetio/THS THF Sl/3a5c 52.5 #DIV/0! #OIV/0! #DlV/0! Pour info (R&D) USADA 0054 k^