INSTRUMENT CONTROL PARAMETERS:

GC MSD

C:\MSDCHEM\1\METHODS\MAN06B_B.M

ontrol Information

Sample Inlet

Injection Source

Injection Location

Use MS

GC

GC/ALS

ALS

Yes

6890 GC METHOD

170 'C (On)
0.00 min

-•EN

Initial temp:
Initial time:
Ramps:

# Rate Final temp Final time

1 3.00 230 0.00

2 30.00 300 4.67

3 O.O(Off)

• Post temp: 'C
Post time: 0.00 min
Run time: 27.00 min

SONT INLET (SPLIT/SPLITLESS)
Mode: Split

initial temp: 280 'C (On)
Pressure: 170.0 kPa (On)
Split ratio: 10:1
Split flow: 13.2 mL/min
Total flow: 17.8 mL/min
Gas saver: Off
Gas type: Helium

"LUMN 1

Capillary Column

Model Number: Agilent 19091Z-008

Max temperature: 325 'C
Nominal length: 17.0 m

• Nominal diameter: 200.00 um
Nominal film thickness: 0.11 um
Mode: constant pressure

• Pressure: 170.0 kPa

Nominal initial flow: 1.3 mL/mm

Average velocity: 59 cm/sec

Inlet: Front Inlet

Outlet: MSD

Outlet pressure: vacuum

•■ONT DETECTOR (NO DET)

■ 'GNAL 1

•■', Data rate: 20 Hz

Type: test plot

Save Data: Off

Zero: 0.0 (Off)

Range :

Fast Peaks: Off

Attenuation:

)LUMN COMP 1

(No Detectors Installed)

Maximum temp: 325 'C.
Equilibration time: 0.50 min

BACK INLET (UNKNOWN)

COLUMN 2

(not installed)

BACK DETECTOR (NO DET)

SIGNAL 2

Data rate: 20 Hz
Type: test plot
Save Data: Off
Zero: 0.0 (Off)
Range:
Fast Peaks: Off
Attenuation:

COLUMN COMP 2

(No Detectors Installed)

iERMAL AUX 2

Use: MSD Transfer Line Heater

USADA 0045

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