f .TST OF COIVTENT

n

SECTION 1 : ADMINISTRATIVE PART

Summary of analyses

Internal chain of custody of sample A and sample A related aliquots

Identification of sample n°995474

Documentation of receipt of intact samples

Analytical deviation

pages 1-22

1

3

IS

20

22

SECTION 2 : TECHNICAL PART

pages 23-173

D

a

2.1. Immunological screening

List of screening analyses, method and preparative form, description of analysis

Screening data

- Sample A995474

2.2. Natural hormone screening

List of screening analyses, method and preparative form, description of analysis
Screening data

- Negative aliquot

- Sample A995474

- Positive ahquot

Data on instnmient performances
Result form

2.3. Second analysis for confinnation of T/E ratio (aliquot with hydrolysis)

List of confirmation analyses, method and preparative form, description of analysis
Confirmation data

- Negative aliquot

- San^le A995474
-Positive aliquot

Data on instrument performances
Result form

23-30

23
30
30

31-64
31
46
46
49
55
58
63

65-92
65
SI

SI
82
85
88
92

[}

0-

LJ

2.4. Confinnation analysis by GC/C/IRMS

List of confirmation analyses, method and preparative form

2.4.1. GC/MS analysis
Description of GC/MS analysis

GC/MS analysis data: Negative ahquot and Sample A995474 for each fraction
Data on instrument performances
Result form

2.4.2. Isotopic ratio analysis
Description of GC/C/KMS analysis

Isotopic ratio analysis data: Negative aliquot and Sample A995474 for each fraction
Data on instrument performances
Result form

93-175
93

113
113
119
135
138
142
142
145
163
174

SECTION 3 : Certificate of analysis n°28423

pages 176-177

ANNEXES

pages 178-207

Reanalysis sheet 178

First analysis for confirmation of T/E ratio according to 2.3 plus an aliquot of sample A995474 without
hydrolysis 179

USADA 0002